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Any part of this Operation Manual cannot be reproduced in any form (as printed matter, photocopies, microfilms or in any other form) or processed, copied or disseminated using electronic system without written consent of Brookfield Viscometers Ltd. Brookfield Viscometers Ltd bears no responsibility for any technical or print technical errors or incomplete information in this Operation Manual. We reserve the right to change this Operation Manual without previous announcement. The reproduction of users’ names, trade names, trade marks and so on in this Operation Manual does not create the necessary prerequisites for their use by anybody; frequently it is a question of protected by law registered trade marks, even if they are not marked as such. . Copyright 1998 by Brookfield Viscometers Ltd 1 Whitehall Estate Flex Meadow Pinnacles West Harlow, Essex U.K. CM19 5TJ . MS-WINDOWS - Copyright by Microsoft . IBM, IBM-PC - Registered trade marks of International Business Machines Corporation All rights reserved Revision 10/9 Brookfield Engineering Labs., Inc. Page 2 M/02-212 CONTENTS I. GENERAL DESCRIPTION 5 I.1 Use of the Rheometer 5 I.2 Measuring Principle 5 II. SYSTEM CONFIGURATION 6 II.1 R/S Rheometer 6 II.2 Measuring Devices 8 II.3 Computer System 8 III. INSTRUMENT INSTALLATION 9 III.1 Stand Mounting 9 III.2 Electrical Connections 10 III.2.1 Temperature Sensor Pt100 10 III.2.2 AC-Adaptor 11 III.2.3 Printer Connection 11 III.2.4 Computer Connection 11 III.3 Mounting of temperature controlled measuring devices 12 III.3.1 Mounting of temp control device FTK-CC with and without cooling device KE 12 III.3.2 Mounting of the measuring device ME-CP/PP 14 III.3.3 Mounting of the cooling device KE 17 IV. ENVIRONMENT, HANDLING, CLEANING AND MAINTENANCE 18 IV.1 Operating environment, Storage 18 IV.2 Handling 18 IV.3 Cleaning 18 IV.4 Maintenance 19 V. MEASURING SYSTEMS 20 V.1 Measurement directly in the substance 20 V.2 Measurement with substance in measuring system 21 V.3 Measurement with temperature control device FTK-CC 22 V.4 Measurement with cone/plate and plate/plate measuring systems 23 VI. OPERATION AND MENUE SYSTEM 25 VI.1 Keyboard 26 VI.2 Menu System of R/S Rheometer 28 VI.3 Selecting from Lists 29 VI.4 Input of numerical values and alphanumeric texts 30 VI.5 Menue entries (MAIN menue) 32 VI.5.1 MAIN-Menue > Run Single 32 VI.5.2 MAIN-Menue > Run Program 34 VI.5.3 MAIN menue > Remote 36 VI.5.4 MAIN menue > Utilities 36 VI.5.5 MAIN menue > Configuration 36 VI.6 Menue entries in the Utilities-Menue 37 VI.6.1Utilities > Zero Calibration 37 VI.6.2 Utilities > Edit Programs 37 VI.6.3 Utilities > Print Programs 41 VI.6.4 Utilities > Measuring systems 41 VI.6.5 Utilities > Print memory 42 VI.6.6 Utilities > Clear memory 43 VI.6.7 Utilities > Measure temperature 43 Brookfield Engineering Labs., Inc. Page 3 M/02-212 VI.7 Menu entries of the CONFIGURATION menu 44 VI.7.1 Configuration > Set output mode 44 VI.7.2 Configuration > MeasCount mode 45 VI.7.3 Configuration > Reset meascount 45 VI.7.4 Configuration > Set Time/Date 45 VI.7.5 Configuration > Set RS232 Parameter 46 VI.7.6 Configuration > Language 47 VI.7.7 Configuration > Service, Service 2 47 VI.8 Serial Data transfer via Interface RS232 47 VII. MEASUREMENTS 50 VII.1 Measuring in manual mode 50 VII.2 Measuring in Remote-mode 51 VIII. TECHNICAL DATA 52 IX. GUARANTEE 54 APPENDIX A1 Data sheets of standard measuring systems 55 A2 Error messages 58 A3 Pin-layout of the serial data cable 61 A4 Requirements to the mains connecting cables 62 A5 Language cross reference 63 Brookfield Engineering Labs., Inc. Page 4 M/02-212 I. General Description I. General Description In this chapter you get general information concerning use and measurement principle of your R/S Rheometer. I.1 Use of the Rheometer The R/S Rheometer system provides possibility of Newtonian fluids viscosity measurements, recording of flow curves as well as determination of viscosity functions of non-Newtonian fluids in steady shear flows. Furthermore, it assures carrying out of measurements in non-stationary shear flows and the measurements of viscoelastic substances values in creep processes. The R/S Rheometer is used in quality control, production control and researches I.2 Measuring Principle The R/S Rheometer is a rotational-shear rate /shear stress-rheometer. Concentric cylinders, measuring cones and plates are available as measuring system. The measuring- sample is positioned in measuring gap between the stationary measuring cup and the rotating measuring bob (Searle-principle), respectively between the rotating cone or plate and the stationary lower plate (cone/plate-, cone/cone-measuring-system). The measuring drive developed for this instrument operates with a high dynamic precision-drive- system with optical encoder without gearing and without mechanical force transducers, so torque is measured without deflection. The R/S Rheometer measuring drive is applicable for carrying out rotational measurements...